Pillay, Adushan; Rousseau, Amanda L.; Fernandes, Manuel A.; De Koning, Charles B.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 38 p. 7809 - 7819
<b>Multi-step reaction with 5 steps<br /> </b>1.1: sodium ethanolate / tetrahydrofuran / 2 h / 0 °C / |Reflux<br />1.2: pH 3<br />2.1: acetic anhydride / 3 h / |Reflux<br />3.1: potassium hydroxide; water / methanol / 6 h / 20 °C<br />4.1: water; potassium carbonate / acetone / 18 h / |Inert atmosphere; |Reflux<br />5.1: neat (no solvent) / 18 h / |Inert atmosphere; |Reflux<br /> <br />
参考文献
Pillay, Adushan; Rousseau, Amanda L.; Fernandes, Manuel A.; De Koning, Charles B. Organic and Biomolecular Chemistry, 2012 , vol. 10, # 38 p. 7809 - 7819
