hydrogen; palladium on activated charcoal in ethanol P=3040 Torr; 18 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;

hydrogen; palladium on activated charcoal 1.) MeOH, room temperature, 2 MPa, 20 min, 2.) MeOH, room temperature, 2 h.; Yield given. Multistep reaction;

1: H2 / 10percent Pd/C / ethanol / 18 h / 3040 Torr 2: 1.) borane*THF complex 2.) HCl / 1.) THF, 60 deg C, 20 h 2.) methanol, reflux, 2 h View Scheme