benzoic acid in neat (no solvent) at 150°C;

in neat (no solvent) byproducts: acetylacetonate; N2 atmosphere, heating (150°C); acac removal (distn.), exces PhCOOH removal (sublimation); elem. anal.;

carbon monoxide; tetra-(n-butyl)ammonium iodide in methanol Electrochem. Process; the solid starting complex is placed in an electrolysis autoclave, the solvent is added under N2, the autoclave is closed, further bubbling of N2 for 30 min, then CO is pressed into the vessel (100 bar), electrolysis (Bu4NI, 293 K, 30 mA, 1.0 V, 120 h); distn., dried over P2O5;

carbon monoxide; lithium perchlorate in methanol Electrochem. Process; the solid starting complex is placed in an electrolysis autoclave, the solvent is added under N2, the autoclave is closed, further bubbling of N2 for 30 min, then CO is pressed into the vessel (100 bar), electrolysis (LiClO4, 293 K, 60 mA, 1.0 V, 195 h);

perchloric acid in N,N-dimethyl-formamide Electrochem. Process; studied at different concentrations of perchloric acid; voltammetry;

in isopropyl alcohol Kinetics; 9-hydroxyquinoline, methanol, 298 K; detected by UV spectra;

(Z)-9-octadecenoic acid in further solvent(s) Fe-compd., oleic acid and oleylamine mixed, stirred, heated at 120°C with vigorous stirring for 2 h, heated to 220°C under Ar, kept at this temp. for 30 min, heated to 300°C at a rate of 2 K*min**-1, kept at 300.gegree.C for 30 min; cooled to room temp., EtOH added, centrifugated, redispersed into hexane, precipitated out by EtOH, dispersed in hexane;

formaldehyd in methanol addn. of metal acetylacetonate into soln. of H2CO in MeOH, heating to 60°C for 20 h under N2; product is trimethylsilylated and analyzed by GC;

anthracene; magnesium in tetrahydrofuran byproducts: MgCl2; addn. of anthracene and EtBr to Mg in THF under Ar, mixt. is stirred for 2-5 h at room temp., addn. of the Fe-salt, stirred for 0.5 h at room temp.; pptn.; filtn., washed (THF), dried (vac.);

in neat (no solvent) heated to 1000°C (5°C/min) in Ar; TGA; XRD;