铂(2+)氯化物-吡啶(1:2:2)合成路线 （共 28 条）
反应条件
1: in water 1 h; Heating / reflux; 2: With hydrogenchloride in water T=4°C; 17 h;
参考文献
VIRGINIA COMMONWEALTH UNIVERSITY
Patent: WO2007/21852 A2, 2007 ;
Location in patent: Page/Page column 17-18 ;
反应条件
pyridine in tetrahydrofuran mixture of pyridine and Pt complex refluxed in THF for 24 h; evapn. in vac., recrystn. (CH2Cl2-hexane); elem. anal.;
参考文献
Goel, Ram G.; Ogini, William O.; Srivastava, Ramesh C.
Inorganic Chemistry, 1981 , vol. 20, p. 3611 - 3616
反应条件
1: water 2: HCl / hydrogenchloride View Scheme
参考文献
Gmelin Handbook: Pt: MVol.D, 78, page 188 - 190
反应条件
in water excess of ligand, stirring and heating for 1 h; according to G. B. Kaufmann, Inorg. Synth. 7 (1963) 249;
参考文献
Tessier, Christian; Rochon, Fernande D.
Inorganica Chimica Acta, 1999 , vol. 295, # 1 p. 25 - 38
反应条件
in dichloromethane Ph3P=CHCO2Me was added to soln. Pt(IV) complex in CH2Cl2, react. mixt. was kept at room temp. for 3 h; solvent was evapd., residue was chromed. on silica using CH2Cl2/Et2O (9:1) as eluent;
参考文献
Wagner; Pakhomova; Bokach; Frausto da Silva; Vicente; Pombeiro; Kukushkin
Inorganic Chemistry, 2001 , vol. 40, # 7 p. 1683 - 1689
反应条件
1: ammonia 2: HCl / hydrogenchloride View Scheme
参考文献
Gmelin Handbook: Pt: MVol.D, 125, page 283 - 285
反应条件
pyridine in water refluxing of K2PtCl4 with excess pyridine until dissoln., addn. to excess concd. aq. NaCl or KCl, heating to 90°C (24 h, pptn.); elem. anal.;
参考文献
Thompson, Laurence K.
Inorganica Chimica Acta, 1980 , vol. 38, p. 117 - 120
反应条件
hydrogen sulfide in water reduction with aq. H2S soln. after storing for several days and shaking;;
参考文献
Joergensen, S. M.
Z. Anorg. Chem., 1900 , vol. 25, p. 353 - 377
Full Text Show Details
Gmelin Handbook: Pt: MVol.D, 265, page 580 - 582
反应条件
1: HCl / hydrogenchloride 2: water 3: hydrogenchloride View Scheme
参考文献
Gmelin Handbook: Pt: MVol.D, 125, page 283 - 285
反应条件
in acetone Pt-complex:pyridine molar ratio was 1:1, 20 °C, 70 h, conversion was 100 percent; monitored by (1)H NMR;
参考文献
De Vekki; Spevak; Skvortsov
Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, 2001 , vol. 27, # 8 p. 579 - 584
