6-硝基-1,2,3,4-四氢喹啉合成路线 （共 17 条）
反应条件
1: sulfuric acid; nitric acid / water / 0.33 h / 0 °C 2: dimethylsulfide borane complex / tetrahydrofuran / 2.17 h / 0 - 80 °C View Scheme
反应条件
1: dinitrogen tetraoxide 2: alcohol / 130 °C / im Rohr View Scheme
参考文献
Chemische Berichte, , vol. 31, p. 2540
反应条件
sulfuric acid; potassium nitrate Erhitzen des Reaktionsprodukts mit wss. Salzsaeure;
参考文献
Canadian Journal of Chemistry, , vol. 30, p. 711,717
反应条件
ethanol; platinum Hydrogenation;
参考文献
Kulka; Manske
Canadian Journal of Chemistry, 1952 , vol. 30, p. 711,717
反应条件
1.1: sodium hydride / mineral oil; dichloromethane / 0.5 h / |Inert atmosphere 1.2: 48 h / 30 °C / |Inert atmosphere 2.1: tin(ll) chloride / ethanol / 22 h / 70 °C View Scheme
参考文献
Compain, Guillaume; Bonneau, Celine; Martin-Mingot, Agnes; Thibaudeau, Sebastien
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4463 - 4472
反应条件
1: 5-nitro-1,2,3,4-tetrahydroquinoline With sodium hydride in dichloromethane; mineral oil 0.5 h; Inert atmosphere; 2: acetyl chloride in dichloromethane; mineral oil T=30°C; 48 h; Inert atmosphere;
参考文献
Compain, Guillaume; Bonneau, Celine; Martin-Mingot, Agnes; Thibaudeau, Sebastien
Journal of Organic Chemistry, 2013 , vol. 78, # 9 p. 4463 - 4472
反应条件
aluminum oxide in N,N-dimethyl-formamide T=120°C; 10 h; Inert atmosphere;
参考文献
Damodara, Dandu; Arundhathi, Racha; Likhar, Pravin R.
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 1 p. 189 - 198
