反应条件
1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 18 h / 0 - 20 °C / |Inert atmosphere 2.1: hydrogenchloride; methanol / water / 6 h / 20 °C 3.1: sodium periodate / water; methanol / 1 h / 0 °C 4.1: sodium tetrahydroborate / water; methanol / 0.5 h / 20 °C 4.2: 3 h / |Reflux 5.1: ammonia / water; methanol / 20 °C View Scheme
参考文献
Kulkarni, Mukund G.; Shaikh, Yunnus B.; Birhade, Deekshaputra R.; Borhade, Ajit S.; Chavhan, Sanjay W.; Dhondge, Attrimuni P.; Gaikwad, Dnyaneshwar D.; Dhatrak, Nagorao R.
Tetrahedron Asymmetry, 2012 , vol. 23, # 17 p. 1234 - 1237
