反应条件
in tetrahydrofuran Fe-complex dissoln. in in situ prepared W-complex soln., solvent removal (water-jet pump, 25°C), ppt. extn. (CH2Cl2), concd. ext. chromy. (SiO2 column, elution with light petroleum ether into several fractions); product eluat boiling down to dryness (vac., 20°C), residue dissoln. (CH2Cl2), heptane addn., soln. vac. concn., keeping at -18°Cfor 2 d, crystals sepn. (decantation), washing (cold heptane), vac. drying;
参考文献
Pasynskii, A. A.; Kolobkov, B. I.; Yandulov, D. V.; Katser, S. B.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1995 , vol. 40, p. 579 - 581
Zhurnal Neorganicheskoi Khimii, 1995 , vol. 40, p. 601 - 603
