反应条件
in tetrahydrofuran N2-atmosphere; refluxing hexacarbonyl with LiCp(*) for 50 h, addn. to Rh-complex, stirring at room temp. for 1 h; water addn., decantation, collection (filtration), washing (water), drying (vac.), extn. into CH2Cl2, filtration, evapn., dissoln. in CH2Cl2, crystn. on layering with pentane (room temp., 3 d), washing (petroleum ether), drying (vac.); elem. anal.;
参考文献
Lindsell, W. Edward; McCullough, Kevin J.; Plancq, Sabine
Journal of Organometallic Chemistry, 1995 , vol. 491, # 1-2 p. 275 - 282