N-((4ar,6r,7r,8r,8as)-6,8-双(苄氧基)-2-苯基六氢吡喃o[3,2-d][1,3]二噁英-7-基)乙酰胺合成路线 (共 7 条)
反应条件
1: sodium hydride / dimethylformamide 2: lithium aluminium hydride / diethyl ether / Ambient temperature 3: pyridinium p-toluenesulphonate / H2O; pyridine / Ambient temperature 4: pyridine 5: mercuric chloride-mercuric oxide 6: sodium hydride / dimethylformamide 7: potassium tert-butoxide / dimethylsulfoxide / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 100, p. C5 - C9
反应条件
1: 6.88 g / NaOMe / methanol / Ambient temperature 2: p-toluenesulphonic acid / acetonitrile / 60 h / 60 °C 3: NaH / tetrahydrofuran View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 70, # 10 p. 2607 - 2617
反应条件
1: 26 percent / Hg(CN)2, HgBr2 2: 6.88 g / NaOMe / methanol / Ambient temperature 3: p-toluenesulphonic acid / acetonitrile / 60 h / 60 °C 4: NaH / tetrahydrofuran View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 70, # 10 p. 2607 - 2617
反应条件
1: p-toluenesulphonic acid / acetonitrile / 60 h / 60 °C 2: NaH / tetrahydrofuran View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 70, # 10 p. 2607 - 2617
反应条件
1: 26 percent / Hg(CN)2, HgBr2 2: 6.88 g / NaOMe / methanol / Ambient temperature 3: p-toluenesulphonic acid / acetonitrile / 60 h / 60 °C 4: NaH / tetrahydrofuran View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 70, # 10 p. 2607 - 2617
13343-61-8N-[(4aR,6R,7R,8R,8aS)-6-苄氧基-8-羟基-2-苯基-4,4A,6,7,8,8A-六氢吡喃并[5,6-d][1,3]二恶英-7-基]乙酰胺+
→
反应条件
sodium hydride in tetrahydrofuran
参考文献
Canadian Journal of Chemistry, , vol. 70, # 10 p. 2607 - 2617
反应条件
hydrogenchloride; 3 A molecular sieve; sodium cyanoborohydride in tetrahydrofuran 0.75 h;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 10 p. 2607 - 2617