in ethanol EtOH soln. of ligand added dropwise to warm EtOH soln. of metal chloride, mixt. stirred for 1 h, cooled to room temp.; filtered off, washed (EtOH), dried (vac.);
in ethanol soln. of 1,10-phenanthroline monohydrate in EtOH added to soln. of ZnCl2in EtOH; after 0.5 h ppt. filtered off; washed (EtOH); dried at room temp. for 0.5 h; elem. anal.;
参考文献
Skogareva; Minacheva; Sergienko; Minaeva; Filippova
Russian Journal of Inorganic Chemistry, 2004 , vol. 49, # 6 p. 853 - 862
