N,N-二甲基-4-甲基苯甲酰胺合成路线 （共 38 条）
反应条件
tert.-butylhydroperoxide; iodine; sodium hydroxide T=70 - 80°C; 24 h;
参考文献
Li, Huamin; Xie, Jin; Xue, Qicai; Cheng, Yixiang; Zhu, Chengjian
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6479 - 6482,4
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water T=90°C; 24 h;
参考文献
Liu, Zhaojun; Zhang, Jie; Chen, Shulin; Shi, Erbo; Xu, Yuan; Wan, Xiaobing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3231 - 3235
反应条件
sodium methylate; nickel diacetate in 1,4-dioxane T=110°C;
参考文献
Ju, Jinhun; Jeong, Miso; Moon, Jeongju; Hyun, Min Jung; Lee, Sunwoo
Organic Letters, 2007 , vol. 9, # 22 p. 4615 - 4618
反应条件
1: para-bromotoluene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Ushijima, Sousuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 24 p. 4701 - 4709
反应条件
sodium methylate; nickel diacetate in 1,4-dioxane T=110°C; 12 h;
参考文献
Ju, Jinhun; Jeong, Miso; Moon, Jeongju; Hyun, Min Jung; Lee, Sunwoo
Organic Letters, 2007 , vol. 9, # 22 p. 4615 - 4618
反应条件
tert.-butylhydroperoxide; Cu(ClO4)2*6H2O in N,N-dimethyl-formamide T=100°C; 15 h; Reagent/catalyst;
参考文献
Kumar, P. Santhosh; Kumar, G. Sathish; Kumar, R. Arun; Reddy, N. Veera; Rajender Reddy
European Journal of Organic Chemistry, 2013 , # 7 p. 1218 - 1222
反应条件
N-ethyl-N,N-diisopropylamine; [bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane T=0°C; 0.5 h;
参考文献
Kangani, Cyrous O.; Kelley, David E.
Tetrahedron Letters, 2005 , vol. 46, # 51 p. 8917 - 8920
反应条件
copper(I) oxide; 1,10-phenanthroline; oxygen; toluene-4-sulfonic acid T=140°C; P=760.051 Torr; 24 h; Sealed tube;
参考文献
Hu, Chenxu; Yan, Xufei; Zhou, Xiangge; Li, Zhengkai
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 47 p. 8179 - 8182
反应条件
hydrogenchloride; tert.-butylhydroperoxide; iodine in cyclohexane; water T=70 - 80°C; 20 h;
参考文献
Gao, Lingfeng; Tang, Haoming; Wang, Zhiyong
Chemical Communications, 2014 , vol. 50, # 31 p. 4085 - 4088
反应条件
Zr(NMe2)4 in toluene T=50°C; 5 h; Inert atmosphere;
参考文献
Stephenson, Nickeisha A.; Zhu, Jiang; Gellman, Samuel H.; Stahl, Shannon S.
Journal of the American Chemical Society, 2009 , vol. 131, # 29 p. 10003 - 10008
