4-氯-N，N-二甲基苯甲酰胺合成路线 （共 33 条）
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water T=90°C; 12 h;
参考文献
Li, Huamin; Xie, Jin; Xue, Qicai; Cheng, Yixiang; Zhu, Chengjian
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6479 - 6482,4
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water T=90°C; 24 h;
参考文献
Liu, Zhaojun; Zhang, Jie; Chen, Shulin; Shi, Erbo; Xu, Yuan; Wan, Xiaobing
Angewandte Chemie - International Edition, 2012 , vol. 51, # 13 p. 3231 - 3235
反应条件
1: 1-chloro-4-bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78 - 20°C; 2 h; 3: methanol Further stages;
参考文献
Ushijima, Sousuke; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 24 p. 4701 - 4709
反应条件
tert.-butylhydroperoxide in acetonitrile T=80°C; 24 h;
参考文献
Ekoue-Kovi, Kekeli; Wolf, Christian
Organic Letters, 2007 , vol. 9, # 17 p. 3429 - 3432
反应条件
tert.-butylhydroperoxide; CuO in water T=85°C; 15 h;
参考文献
Priyadarshini; Amal Joseph; Lakshmi Kantam
RSC Advances, 2013 , vol. 3, # 40 p. 18283 - 18287
反应条件
bis(di-tert-butylphosphinous acid)PdCl2 in acetonitrile T=50°C; 24 h;
参考文献
Ekoue-Kovi, Kekeli; Wolf, Christian
Organic Letters, 2007 , vol. 9, # 17 p. 3429 - 3432
反应条件
triethylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Das, Shoubhik; Addis, Daniele; Zhou, Shaolin; Junge, Kathrin; Beller, Matthias
Journal of the American Chemical Society, 2010 , vol. 132, # 6 p. 1770 - 1771
反应条件
magnesium methanolate in methanol T=80°C; 72 h; Inert atmosphere;
参考文献
Bundesmann, Mark W.; Coffey, Steven B.; Wright, Stephen W.
Tetrahedron Letters, 2010 , vol. 51, # 30 p. 3879 - 3882
反应条件
hydrogenchloride; tert.-butylhydroperoxide; iodine in cyclohexane; water T=70 - 80°C; 20 h;
参考文献
Gao, Lingfeng; Tang, Haoming; Wang, Zhiyong
Chemical Communications, 2014 , vol. 50, # 31 p. 4085 - 4088
反应条件
1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate in tetrachloromethane; water T=20°C; Inert atmosphere;
参考文献
Baba, Haruka; Moriyama, Katsuhiko; Togo, Hideo
Synlett, 2012 , vol. 23, # 8 p. 1175 - 1180
