hydroxylamine hydrochloride in N,N-dimethyl-formamide T=110°C; 8 h;

1.1: hydroxylamine hydrochloride / N,N-dimethyl-formamide / 6 h / 60 °C / |Inert atmosphere 1.2: 18 h / 130 °C 2.1: sodium hydroxide / ethanol / 15 h / 20 °C 2.2: 2 h / |Reflux 3.1: acetic anhydride / 4 h / 20 °C 4.1: ammonium formate / formamide / 6 h / 160 °C / |Inert atmosphere 5.1: trichlorophosphate / 2 h / |Inert atmosphere; |Reflux View Scheme

1: hydroxylamine chloride / ethanol 2: Ac2O View Scheme

potassium carbonate in acetonitrile 0.0833333 h; microwave irradiation;

(i) MeOH, (ii) /BRN= 2440490/; Multistep reaction;

1: NH2OH*HCl / dimethylformamide / 8 h / 110 °C 2: Ac2O / 18 h / Heating View Scheme

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '956581', constants.ctx, '0')">trichlorophosphate</a> <br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '956581', constants.ctx, '0')">trichlorophosphate</a> <br />T=60&deg;C;&nbsp;Vilsmeier-Haack reaction;&nbsp;3&nbsp;h;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '956581', constants.ctx, '0')">trichlorophosphate</a> <br /> <br /> &nbsp;