(E)-1-苯基-2-M-甲苯基乙烯合成路线 (共 48 条)
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; Heck reaction; 12 h; Inert atmosphere; regioselective reaction;
参考文献
Liu, Hongqiang; Wang, Lei; Li, Pinhua
Synthesis, 2008 , # 15 art. no. F04908SS, p. 2405 - 2411
反应条件
[PdCl(C3H5){P(OCMe2CMe2O)OCH2CMe2NH2}]; tetrabutylammomium bromide; caesium carbonate in N,N-dimethyl-formamide T=140°C; Heck reaction; 4 h; Inert atmosphere; stereoselective reaction;
参考文献
Shaikh, Tanveer Mahamadali; Hong, Fung-E
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1578 - 1588
反应条件
PdCl2{P(OCMe2CMe2O)OCH2CMe2NH2}; tetrabutyl ammonium fluoride in N,N-dimethyl-formamide T=140°C; Hiyama coupling; 4 h; Inert atmosphere; stereoselective reaction;
参考文献
Skarynska, Anna; Gniewek, Andrzej
Journal of Organometallic Chemistry, 2011 , vol. 696, # 18 p. 2985 - 2992
反应条件
N-bromosuccinmide; palladium diacetate in toluene T=20°C; Heck Reaction; 12 h; Inert atmosphereSchlenk technique;
参考文献
Shaikh, Tanveer Mahamadali; Hong, Fung-E
Beilstein Journal of Organic Chemistry, 2013 , vol. 9, p. 1578 - 1588
反应条件
C18H19Cl2N2PPd; triethylamine in N,N-dimethyl-formamide T=140°C; Heck Reaction; 21 h; Inert atmosphereSchlenk technique;
参考文献
Suarez-Meneses, Jesus V.; Bonilla-Reyes, Edgar; Ble-Gonzalez, Ever A.; Ortega-Alfaro, M. Carmen; Toscano, Ruben Alfredo; Cordero-Vargas, Alejandro; Lopez-Cortes, Jose G.
Tetrahedron, 2014 , vol. 70, # 7 p. 1422 - 1430
反应条件
SIDip*HCl; palladium diacetate in tetrahydrofuran T=20°C; Sizuki-Miyaura cross coupling; 3.5 h;
参考文献
Andrus; Song
Organic letters, 2001 , vol. 3, # 23 p. 3761 - 3764
反应条件
DHEABTBAB; palladium diacetate T=100°C; Heck reaction; 6 h; Inert atmosphere; stereoselective reaction;
参考文献
Keesara, Srinivas; Parvathaneni, Saiprathima; Dussa, Govardhan; Mandapati, Mohan Rao
Journal of Organometallic Chemistry, 2014 , vol. 765, p. 31 - 38
反应条件
isoquinoline; lithium chloride; palladium dichloride in various solvent(s) T=160°C;
参考文献
Goossen, Lukas J.; Paetzold
Angewandte Chemie - International Edition, 2002 , vol. 41, # 7 p. 1237 - 1241
反应条件
tert.-butylnitrite; chloroacetic acid; bis(dibenzylideneacetone)-palladium(0) in acetic acid T=50°C; 0.5 h;
参考文献
Kikukawa, Kiyoshi; Maemura, Koji; Kiseki, Yasuyuki; Wada, Fumio; Matsuda, Tsutomu; Giam, Choo S.
Journal of Organic Chemistry, 1981 , vol. 46, # 24 p. 4885 - 4888
反应条件
palladium diacetate; SIDip*HCl in tetrahydrofuran T=20°C; Mizoroki-Heck coupling; 5 h;
参考文献
Andrus, Merritt B.; Song, Chun; Zhang, Jiuqing
Organic Letters, 2002 , vol. 4, # 12 p. 2079 - 2082