(E)-1-苯基-2-M-甲苯基乙烯合成路线 （共 48 条）
反应条件
1: tetrahydrofuran / 2 h / Heating 2: pyridine, POCl3 / 2 h / Heating View Scheme
参考文献
Yueh, Wang; Bauld, Nathan L.
Journal of the American Chemical Society, 1995 , vol. 117, # 21 p. 5671 - 5676
反应条件
1: tetrahydrofuran / 2 h / Heating 2: pyridine, POCl3 / 2 h / Heating View Scheme
参考文献
Yueh, Wang; Bauld, Nathan L.
Journal of the American Chemical Society, 1995 , vol. 117, # 21 p. 5671 - 5676
反应条件
1: phenylmethylphosphonic acid,diethyl ester With 18-crown-6 ether; sodium methylate in N,N-dimethyl-formamide T=20°C; 0.0833333 h; 2: 3-methyl-benzaldehyde in N,N-dimethyl-formamide T=20 - 120°C; Horner-Emmons-Wadsworth reaction; 6 h;
参考文献
Heynekamp, Justin J.; Weber, Waylon M.; Hunsaker, Lucy A.; Gonzales, Amanda M.; Orlando, Robert A.; Deck, Lorraine M.; Vander Jagt, David L.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 24 p. 7182 - 7189
反应条件
pyridine; zinc; NiCl2((PPh3)P)2 in acetonitrile T=65°C; 4 h;
参考文献
Lebedev, S. A.; Lopatina, V. S.; Sorokina, R. S.; Berestova, S. S.; Petrov, E. S.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 11 p. 2329 - 2332
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 11 p. 2508 - 2511
反应条件
triethyl phosphite in tetrahydrofuran
参考文献
Ho, Tong-Ing; Chang, Cheu-Ming; Wang, Sen Ren; Cheng, Cheu Pyeng
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 123 - 128
反应条件
lithium ethanolate in ethanol Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ito, Yoshikatsu; Uozu, Yoshihiro; Dote, Toshimichi; Ueda, Masahiro; Matsuura, Teruo
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 189 - 198
反应条件
in tetrahydrofuran T=0°C; 1 h;
参考文献
Huang, Xian; Xu, Xin-Hua
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 20 p. 3321 - 3322
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; Heck reaction; 2 h; optical yield given as percent de;
参考文献
Wan, Li; Cai, Chun
Transition Metal Chemistry, 2011 , vol. 36, # 7 p. 747 - 750
反应条件
diiron nonacarbonyl; tributylphosphine; 4-bromooctafluorobutanetriethoxysilane in tetrahydrofuran T=60°C; 48 h; Inert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Enthaler, Stephan; Haberberger, Michael; Irran, Elisabeth
Chemistry - An Asian Journal, 2011 , vol. 6, # 6 p. 1613 - 1623
反应条件
methylethyl sulfide; palladium diacetate; silver carbonate; 2,2,2-trimethylacetic acid T=120°C; Heck type coupling reaction; 8 h; Inert atmosphere;
参考文献
Li, Hu; He, Ke-Han; Liu, Jia; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Shi, Zhang-Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7028 - 7030
