(E)-1-苯基-2-M-甲苯基乙烯合成路线 （共 48 条）
反应条件
pyridine; trichlorophosphate 2 h; Heating;
参考文献
Yueh, Wang; Bauld, Nathan L.
Journal of the American Chemical Society, 1995 , vol. 117, # 21 p. 5671 - 5676
反应条件
1: 63 percent / NaHCO3 / FeCl2*4H2O / acetone; H2O / -25 - 20 °C / pH 4 - 6 2: 95 percent / KOH / methanol / 0.5 h / Heating View Scheme
参考文献
Obushak
Russian Journal of General Chemistry, 1998 , vol. 68, # 3 p. 443 - 445
反应条件
C27H21F3N6OPd; tetrabutylammomium bromide; sodium acetate T=140°C; Heck reaction; 12 h; Inert atmosphere;
参考文献
Sie, Ming-Han; Hsieh, Yuan-Hsin; Tsai, Yi-Hua; Wu, Jia-Rong; Chen, Shih-Jung; Kumar, P. Vijaya; Lii, Jenn-Huei; Lee, Hon Man
Organometallics, 2010 , vol. 29, # 23 p. 6473 - 6481
反应条件
1.1: toluene / 0.17 h / 110 °C / Inert atmosphere 1.2: 0.08 h / 110 °C / Inert atmosphere 1.3: 110 °C / Inert atmosphere 2.1: [PdCl2P(OCH2CMe2NH)OCH2CMe2NH2]; tetrabutyl ammonium fluoride / N,N-dimethyl-formamide / 4 h / 140 °C / Inert atmosphere View Scheme
参考文献
Skarynska, Anna; Majchrzak, Mariusz; Trzeciak, Anna M.; Marciniec, Bogdan
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 351, p. 128 - 135
反应条件
4,4'-di-tert-butylbiphenyl; lithium; nickel dichloride in tetrahydrofuran Wittig type olefination reaction; 8 h; RefluxInert atmosphere; optical yield given as percent de;
参考文献
Alonso, Francisco; Riente, Paola; Yus, Miguel
Synlett, 2009 , # 10 p. 1579 - 1582
反应条件
1: 95 percent / NiCl2(PPh3)2 / tetrahydrofuran / 3 h / Ambient temperature 2: 88 percent / NiCl2(PPh3)2 / tetrahydrofuran / 48 h / Ambient temperature View Scheme
参考文献
Zhu, Liu-Sheng; Huang, Xian
Synthetic Communications, 1997 , vol. 27, # 1 p. 39 - 44
反应条件
1: triethylamine; triphenylphosphine; palladium dichloride / 1,4-dioxane / 72 h / 60 °C 2: diiron nonacarbonyl; tributylphosphine; 4-bromooctafluorobutanetriethoxysilane / tetrahydrofuran / 48 h / 60 °C / Inert atmosphere View Scheme
参考文献
Enthaler, Stephan; Haberberger, Michael; Irran, Elisabeth
Chemistry - An Asian Journal, 2011 , vol. 6, # 6 p. 1613 - 1623
反应条件
1: sodium hydride / N,N-dimethyl-formamide / 2 h / -20 - 20 °C 2: diethylaluminium chloride / hexane; 1,4-dioxane / 4 h / 20 °C View Scheme
参考文献
Sarkar, Satinath; Jana, Manoranjan; Tadigoppula, Narender
RSC Advances, 2013 , vol. 3, # 41 p. 18755 - 18758
反应条件
1: 1.) CpZr(H)Cl / 1.) THF, r.t., 20 min, 2.) THF, r.t., 4.0 h 2: 76 percent / tetrahydrofuran / 1 h / 0 °C View Scheme
参考文献
Huang, Xian; Xu, Xin-Hua
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 20 p. 3321 - 3322
反应条件
(i), (ii) aq. H2SO4; Multistep reaction;
参考文献
Mallory,F.B.; Mallory,C.W.
Journal of the American Chemical Society, 1972 , vol. 94, # 17 p. 6041 - 6048
