(E)-1-苯基-2-M-甲苯基乙烯合成路线 （共 48 条）
反应条件
1: caesium carbonate; tris-(dibenzylideneacetone)dipalladium(0); trifuran-2-yl-phosphane / 1,4-dioxane; water / 65 °C / |Inert atmosphere 2: bis-triphenylphosphine-palladium(II) chloride; sodium tetrahydroborate; N,N,N',N,-tetramethylethylenediamine / tetrahydrofuran / 10 h / 25 °C / |Inert atmosphere View Scheme
参考文献
Chelucci, Giorgio
Chemical Communications, 2014 , vol. 50, # 31 p. 4069 - 4072
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; copper (II) acetate monohydrate; trichloroacetic acid T=120°C; 22 h; regioselective reaction;
参考文献
Zheng, Lu; Wang, Jianhui
Chemistry - A European Journal, 2012 , vol. 18, # 31 p. 9699 - 9704
反应条件
iron(II) chloride 2.) acetone, 20 - 30 deg C; Yield given. Multistep reaction;
参考文献
Obushak, N. D.; Lyakhovich, M. B.; Ganushchak, N. I.; Bilaya, E. E.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 7 p. 1391 - 1392
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1545
参考文献
Bergmann; Schapiro
Journal of Organic Chemistry, 1947 , vol. 12, p. 57,63
反应条件
(i) Mg, Et2O, (ii) /BRN= 741964/, (iii) aq. H2SO4; Multistep reaction;
参考文献
Abenhaim,D. et al.
Bulletin de la Societe Chimique de France, 1972 , p. 985 - 990
反应条件
[bis(acetoxy)iodo]benzene in 1,4-dioxane T=20°C; 8 h; Air atmosphereIrradiation;
参考文献
Li, Hu; He, Ke-Han; Liu, Jia; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Shi, Zhang-Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7028 - 7030
参考文献
Laarhoven,W.H. et al.
Tetrahedron, 1970 , vol. 26, p. 4865 - 4881
反应条件
[bis(acetoxy)iodo]benzene in 1,4-dioxane
T=20°C; 8 h; Air atmosphereIrradiation;
参考文献
Li, Hu; He, Ke-Han; Liu, Jia; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Shi, Zhang-Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7028 - 7030
