(3S,5E,7E,14Xi)-3-{[二甲基(2-甲基-2-丙基)硅烷基]氧基}-9,10-开链胆甾-5,7,10-三烯-25-醇合成路线 (共 2 条)
反应条件
1: sulfur dioxide / Reflux 2: 1H-imidazole / N,N-dimethyl-formamide 3: sodium hydrogencarbonate / ethanol / Reflux View Scheme
参考文献
Ray, Rahul; Lambert, James R.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 8 p. 2537 - 2540
反应条件
1: SeO2, N-methylmorpholine N-oxide / methanol; CH2Cl2 / Heating 2: acridine / Irradiation 3: (C4H9)4N1+*F1- / tetrahydrofuran View Scheme
参考文献
Andrews; Barton; Cheng; et al.
Journal of Organic Chemistry, 1986 , vol. 51, # 9 p. 1635 - 1637