in dichloromethane (Ar), at -40/-50°C for 15-25 min; degassed (vac., -78°C), phases sepd., solid washed with CH2Cl2, exts. combined; not isolated, detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 598, # 1 p. 127 - 135
in dichloromethane (Ar), at -40/-50°C for 15-25 min; degassed (vac., -78°C), phases sepd., solid washed with CH2Cl2, exts. combined; not isolated, detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 598, # 1 p. 127 - 135
in dichloromethane (Ar), at -40/-50°C for 15-25 min; degassed (vac., -78°C), phases sepd., solid washed with CH2Cl2, exts. combined; not isolated, detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 598, # 1 p. 127 - 135
in dichloromethane (Ar), at -40/-50°C for 15-25 min; degassed (vac., -78°C), phases sepd., solid washed with CH2Cl2, exts. combined; not isolated, detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 598, # 1 p. 127 - 135
in dichloromethane (Ar), at -40/-50°C for 15-25 min; degassed (vac., -78°C), phases sepd., solid washed with CH2Cl2, exts. combined; not isolated, detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 598, # 1 p. 127 - 135
in dichloromethane (Ar), at -40/-50°C for 15-25 min; degassed (vac., -78°C), phases sepd., solid washed with CH2Cl2, exts. combined; not isolated, detected by NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 598, # 1 p. 127 - 135
in methanol; water KHF2 dissolved in aq. MeOH, B(OMe)3 added by stirring; after 1 h decanted, pptd. dissolved in water allowed to stand 4 d, detected by 19F NMR spectra; final molar ratio of (BF3OMe)(1-) to (BF4)(1-) 96:1;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 627, # 11 p. 2499 - 2505
in further solvent(s) PF6 salt dissolved in propylene carbonate and LiBF4 dissolved in dimethyl carbonate, solns. mixed in various ratio (1.0-2.0); filtered, washed with Et2O, monitored by 19F NMR spectra;
参考文献
Zeitschrift fur Anorganische und Allgemeine Chemie, , vol. 631, # 10 p. 1840 - 1842
