反应条件
1: 70 percent / Et3N / toluene / 6 h / Heating 2: 73 percent / 2 N HCl / 5 h / Heating 3: 1.) LiAlH4, 2.) aq. NaOH / 1.) Et2O, reflux, 3 h, 2.) Et2O, RT, 30 min View Scheme
参考文献
Giannangeli, Marilena; Cazzolla, Nicola; Luparini, Maria Rita; Magnani, Maurizio; Mabilia, Massimo; Picconi, Giuseppe; Tomaselli, Mauro; Baiocchi, Leandro
Journal of Medicinal Chemistry, 1999 , vol. 42, # 3 p. 336 - 345
