1-(1-环庚烯-1-基)吡咯烷合成路线 （共 15 条）
反应条件
lead(IV) acetate; boron trifluoride diethyl etherate in benzene 30 h; Ambient temperature;
参考文献
Cekovic, Z.; Bosnjak, J.; Cvetkovic, M
Tetrahedron Letters, 1980 , vol. 21, p. 2675 - 2678
反应条件
in toluene T=-50°C; 2 h;
参考文献
Hayakawa, Kenji; Takewaki, Makoto; Fujimoto, Ichiro; Kanematsu, Ken
Journal of Organic Chemistry, 1986 , vol. 51, # 26 p. 5100 - 5105
反应条件
ammonium hydroxide; water 1) 1 h, CH2Cl2, -70 deg C, 2) 0 deg C, pH= 12; Yield given. Multistep reaction;
参考文献
Risch, Nikolaus; Esser, Achim
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 2 p. 208 - 210
反应条件
ammonium hydroxide; water 1) 1 h, DMF, -60 deg C, 2) 0 deg C, pH= 12; Yield given. Multistep reaction;
参考文献
Risch, Nikolaus; Esser, Achim
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 2 p. 208 - 210
反应条件
ammonium hydroxide; water 1) 1 h, THF, -70 deg C, 2) 0 deg C, pH= 12; Yield given. Multistep reaction;
参考文献
Risch, Nikolaus; Esser, Achim
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 2 p. 208 - 210
反应条件
(i) dioxane, (ii) aq. HCl; Multistep reaction;
参考文献
Opitz,G. et al.
Justus Liebigs Annalen der Chemie, 1961 , vol. 649, p. 47 - 57
反应条件
in toluene 14 h; Heating; Yields of byproduct given;
参考文献
Suschitzky, Hans; Wakefield, Basil J.; Whitten, Jeffrey P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2709 - 2716
反应条件
1.1: 1,4-dioxane / |Inert atmosphere; |Reflux 2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C 2.2: 0.5 h / 20 °C View Scheme
参考文献
Fink, Michael J.; Rial, Daniela V.; Kapitanova, Petra; Lengar, Alenka; Rehdorf, Jessica; Cheng, Qiong; Rudroff, Florian; Mihovilovic, Marko D.
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 18 p. 3491 - 3500
反应条件
in chloroform
T=45°C; 16 h;
参考文献
Boger, Dale L.; Panek, James S.
Journal of Organic Chemistry, 1981 , vol. 46, # 10 p. 2179 - 2182
反应条件
1,4-dioxane; triethylamine
anschliessend Behandeln mit wss. HCl;
参考文献
Kuehne
Journal of the American Chemical Society, 1959 , vol. 81, p. 5400,5403
