反应条件
sodium in tetrahydrofuran byproducts: KCl, NaCl; slight stoich. excess of Na, 1100 psi CO, 280°C, 40 h; cooling to room temp., filtration (celite), washing (hot Me2CO), evapn.,dissoln. in hot Me2CO, pptn. on MeOH addn., standing (-15°C, ove rnight), filtration;
参考文献
Klahn, A. Hugo; Oelckers, Beatriz; Toro, Adriana; Godoy, Fernando
Journal of Organometallic Chemistry, 1997 , vol. 548, # 2 p. 121 - 122
