(E)-3,7-二甲基-2,6-辛二烯醛合成路线 (共 128 条)
反应条件
tin; dihydrogen peroxide in various solvent(s) T=100°C; Baeyer-Villiger oxidation; 1 h; Product distribution; Further Variations:SolventsTemperaturesReagents;
参考文献
Corma, Avelino; Iborra, Sara; Mifsud, Maria; Renz, Michael
Journal of Catalysis, 2005 , vol. 234, # 1 p. 96 - 100
反应条件
sodium cyanide; manganese(IV) oxide; acetic acid T=20°C; 20 h;
参考文献
Comeskey, Daniel J.; Rowan, Daryl D.; Matich, Adam J.
Journal of Labelled Compounds and Radiopharmaceuticals, 2006 , vol. 49, # 1 p. 47 - 54
反应条件
sodium hydride 2) THF, RT; Multistep reaction;
参考文献
Gaebler, Andreas; Boland, Wilhelm; Preiss, Ute; Simon, Helmut
Helvetica Chimica Acta, 1991 , vol. 74, # 8 p. 1773 - 1789
反应条件
sodium dithionite; 5α-cholestan-3-one; sodium hydrogencarbonate in 1,4-dioxane T=50°C;
参考文献
Dhillon, Ranjit S.; Singh, Rupinder P.; Kaur, Daljit
Tetrahedron Letters, 1995 , vol. 36, # 7 p. 1107 - 1108
反应条件
hydrogen; monoaluminum phosphate; palladium matal-containing silica-supported catalyst in tetrahydrofuran T=29.9°C; P=3102.9 Torr; Ea, ΔH, ΔS; other Pd support, also in the presence of FeCl2; other solvents, var. pressure and temp.; Thermodynamic dataProduct distribution;
参考文献
Aramendia; Borau; Jimenez; Marinas; Porras; Urbano
Journal of Catalysis, 1997 , vol. 172, # 1 p. 46 - 54
反应条件
hydrogen in isopropyl alcohol T=70°C;
参考文献
Bernas, Heidi; Simakova, Irina; Prosvirin, Igor P.; Maeki-Arvela, Paeivi; Leino, Reko; Murzin, Dmitry Yu
Catalysis Letters, 2012 , vol. 142, # 6 p. 690 - 697
反应条件
acetic acid in ethanol; water electrolysis at copper cathode; further mixtures of solvents: H2O-DMF, H2O-i-PrOH, DMF-EtOH, DMF-MeOH; Product distribution;
参考文献
Russian Chemical Bulletin, , vol. 45, # 1 p. 74 - 78
反应条件
2: 6 h / 150 - 155 °C 3: H2 / PtO2 View Scheme
参考文献
Venuto,P.B.; Day,A.R.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2735 - 2739
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; benzoic acid; (S)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine in chloroform T=-20°C; 63 h; Title compound not separated from byproducts;
参考文献
Hall, Melanie; Stueckler, Clemens; Kroutil, Wolfgang; Macheroux, Peter; Faber, Kurt
Angewandte Chemie - International Edition, 2007 , vol. 46, # 21 p. 3934 - 3937
反应条件
β-D-glucopyranose; glucose dehydrogenase 102; Pichia stipitis OYE 2.6-GST fusion protein, OYE: old yellow enzyme, GST: glutathione S-transferase; NADPH; potassium hydroxide in ethanol T=20°C; pH=7.5; aq. phosphate bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
Bougioukou, Despina J.; Walton, Adam Z.; Stewart, Jon D.
Chemical Communications, 2010 , vol. 46, # 45 p. 8558 - 8560