(E)-3,7-二甲基-2,6-辛二烯醛合成路线 (共 128 条)
反应条件
bis(acetylacetonate)oxovanadium; 2,2'-azo-bisisobutyronitrile; oxygen; 2-methyl-3-ethoxycarbonyl-5-ethylidene-4,5-dihydrofuran in benzene
T=60°C; 18 h;
参考文献
Scettri, Arrigo; Bonadies, Francesco; Lattanzi, Alessandra; Palombi, Laura; Pesci, Silvia
Tetrahedron, 1997 , vol. 53, # 50 p. 17139 - 17150
反应条件
sodium hydroxide; dipotassium peroxodisulfate; nickel sulphate in dichloromethane; water
24 h; Ambient temperature; Yields of byproduct given;
参考文献
Yamazaki, Shigekazu; Yamazaki, Yasuyuki
Chemistry Letters, 1989 , p. 1361 - 1364
反应条件
[2,2']bipyridinyl; 1,10-phenanthroline; di-tert-butylazodicarboxylate; potassium carbonate; copper(l) chloride in toluene
T=35°C; P=15514.9 Torr; 10 h; Autoclave;
参考文献
Liu, Yu; Ma, Shengming
Chinese Journal of Chemistry, 2012 , vol. 30, # 1 p. 29 - 34
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Nuzillard, Jean-Marc; Boumendjel, Ahcene; Massiot, Georges
Tetrahedron Letters, 1989 , vol. 30, # 29 p. 3779 - 3780
反应条件
trimethylamine-N-oxide in dichloromethane; dimethyl sulfoxide
0.5 h; -20 to 0 deg C;
参考文献
Godfrey; Ganem
Tetrahedron Letters, 1990 , vol. 31, # 34 p. 4825 - 4826
反应条件
benzoic acid; bis(2-methylpropenyl)(1,2-bis(diphenylphosphino)ethane)ruthenium in toluene
1.) 70 deg C, 2 h, 2.) 100 deg C, 15 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Picquet, Michel; Bruneau, Christian; Dixneuf, Pierre H.
Chemical Communications, 1997 , # 13 p. 1201 - 1202
反应条件
(1,4-bis(diphenylphosphino)butane)bis(.eta.(3)-2-methylallyl)ruthenium(II) in toluene
参考文献
Picquet, Michel; Bruneau, Christian; Dixneuf, Pierre H.
Chemical Communications, 1997 , # 13 p. 1201 - 1202
反应条件
C56H82N8O20S2 in benzene
T=20°C; 2.5 h; UV-irradiation; optical yield given as percent de;
参考文献
Tsuboi, Takaaki; Takaguchi, Yutaka; Tsuboi, Sadao
Heteroatom Chemistry, 2009 , vol. 20, # 1 p. 1 - 11
反应条件
potassium trichromate(VI) in acetonitrile
24 h;
参考文献
Carlsen, P. H. J.; Kjaerstad, Cathrine; Aasboe, Kari
Acta Chemica Scandinavica, 1995 , vol. 49, # 2 p. 152 - 154
反应条件
pyridinium chlorochromate in dichloromethane
18 h; Heating;
参考文献
Cossy, Janine; Bouzbouz, Samir; Lachgar, Mohamed; Hakiki, Abdelhak; Tabyaoui, Badia
Tetrahedron Letters, 1998 , vol. 39, # 17 p. 2561 - 2564