1: With pyridine Heating; 2: With pyridine; thionyl chloride in benzene T=60°C;
参考文献
Konkel, Michael J.; Wetzel, John M.; Cahir, Marie; Craig, Douglas A.; Noble, Stewart A.; Gluchowski, Charles
Journal of Medicinal Chemistry, 2005 , vol. 48, # 8 p. 3076 - 3079
in water org. ligand addn. to cooled (ice) Rh-salt soln., rhodium removal (filtration), soln. leaving for several d at room temp., pptn. on satd. NaClO4 soln. addn.; ppt. sepn. (filtration), washing (alcohol, ether), air drying; elem. anal.;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 26, p. 77 - 81
Zhurnal Neorganicheskoi Khimii, , vol. 26, p. 147 - 155
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反应条件
in water org. ligand addn. to Rh-salt soln., reaction mixt. heating (water bath, 5 min), rhodium removal (filtration), pptn. from soln.; recrystn. (hot water); elem. anal.;
参考文献
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), , vol. 26, p. 77 - 81
Zhurnal Neorganicheskoi Khimii, , vol. 26, p. 147 - 155