1,1,3,3-四甲基-1-丁硫醇合成路线 （共 4 条）
反应条件
aluminium trichloride; hydrogen sulfide in dichloromethane T=-5 - 0°C; 2 h;
参考文献
Alfer'ev, I. S.; Mikhalin, N. V.; Kotlyarevskii, I. L.; Vainer, L. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 4 p. 786 - 791
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 4 p. 860 - 864
反应条件
(i) Na2S, sulfur, DMSO, (ii) Al-Hg, H2O, THF; Multistep reaction;
参考文献
Kornblum,N.; Widmer,J.
Journal of the American Chemical Society, 1978 , vol. 100, p. 7086 - 7088
反应条件
aluminium trichloride; hydrogen sulfide
参考文献
Pure Oil Co.
Patent: US2531602 , 1946 ;
反应条件
dihydrogen peroxide; sodium iodide in ethyl acetate T=20°C; 24 h;
参考文献
Kirihara, Masayuki; Asai, Yasutaka; Ogawa, Shiho; Noguchi, Takuya; Hatano, Akihiko; Hirai, Yoshiro
Synthesis, 2007 , # 21 art. no. F15107SS, p. 3286 - 3289
