1: 2,2-Dimethyl-[1,3]dioxane-4,6-dione; butyryl chloride With pyridine in dichloromethane T=20°C; 2 h; 2: methanol in dichloromethane 2 h; Further stages.;
参考文献
Teng, Xin; Keys, Heather; Jeevanandam, Arumugasamy; Porco Jr., John A.; Degterev, Alexei; Yuan, Junying; Cuny, Gregory D.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 24 p. 6836 - 6840
Sin, Hong-Sig; Um, Soo-Jong; Rho, Young-Soy; Park, Si-Ho; Kwon, Youn-Ja; Park, Myoung-Soon; Han, Hye-Sook; Kim, So-Mi; Kim, Dong-Myong; Oh, Deon-Kun; Park, Jong-Sup; Bae, Tae-Sung
Patent: US2003/171339 A1, 2003 ;