4-辛基-4H-二噻吩并[3,2-b:2,3-d]吡咯合成路线 (共 2 条)
反应条件
Pd2dba3*CH2Cl2; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate in toluene T=110°C; Buchwald-Hartwig reaction; 7 h; Product distribution; Further Variations:ReagentsSolventsTemperaturesconcentration;
参考文献
Koeckelberghs, Guy; De Cremer, Lieven; Vanormelingen, Wouter; Dehaen, Wim; Verbiest, Thierry; Persoons, Andre; Samyn, Celest
Tetrahedron, 2005 , vol. 61, # 3 p. 687 - 691
反应条件
1: NBS / dimethylformamide / 2 h / Cooling 2: copper powder / dimethylformamide / 2 h / Heating View Scheme
参考文献
Ogawa, Katsu; Rasmussen, Seth C.
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2921 - 2928