反应条件
in hydrogen fluoride HF (liquid); treatment AgF with BF3 in HF, pptn. of AgBF4, adnn. of F2, removal of volatiles, addn. of Hf, BF3 and xenon (condensed in reactor, -100°C), warming to 20°C with stirring (thermal cycling repeated 3-4 times, in 2 h); removal of volatile (vac., -45°C, 5 h), XeF2 (U trap, -78°C); x-ray photography;
参考文献
Zemva, Boris; Hagiwara, Rika; Casteel Jr., William J.; Lutar, Karel; Jesih, Adolf; Bartlett, Neil
Journal of the American Chemical Society, 1990 , vol. 112, # 12 p. 4846 - 4849
