反应条件
1: 89 percent / LiAlH4 / tetrahydrofuran / 1 h / 0 °C
2: 1.) CH3SO2Cl, Et3N, 2.) Bu4NN3 / 1.) CH2Cl2, -50 deg C, 1 h, 2.) THF, 9 h
View Scheme
参考文献
Pearson, William H.; Walavalkar, Rajesh; Schkeryantz, Jeffrey M.; Fang, Wen-Kui; Blickensdorf, James D.
Journal of the American Chemical Society, 1993 , vol. 115, # 22 p. 10183 - 10194
