环己烯-1-硼酸频哪醇酯合成路线 （共 19 条）
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=115°C; 24 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 46, # 6 p. 907 - 909
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2 in cyclohexane T=70°C; 16 h; Inert atmosphere; chemoselective reaction;
参考文献
Dalton Transactions, , vol. 42, # 3 p. 746 - 752
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine in cyclohexane T=70°C; 16 h; Inert atmosphere; chemoselective reaction;
参考文献
Dalton Transactions, , vol. 42, # 3 p. 746 - 752
反应条件
[RhCl(cod)]2; Xantphos in tetrahydrofuran 115°, 24 h, cyclohexene (1.2 equiv.), (RhCl(cod))2 (1.3 molpercent), Xantphos (2.5 molpercent); column purifn.; 1H NMR;
参考文献
Chemical Communications, , vol. 46, # 6 p. 907 - 909
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; 1,3-bis-(diphenylphosphino)propane in chloroform-d1
参考文献
Letters in Organic Chemistry, , vol. 9, # 4 p. 257 - 262
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; tris-(o-tolyl)phosphine in N,N-dimethyl-formamide T=60°C; Suzuki-Miyaura coupling; 0.0833333 h; Inert atmosphere;
参考文献
Doi, Hisashi; Ban, Ikuya; Nonoyama, Akihito; Sumi, Kengo; Kuang, Chunxiang; Hosoya, Takamitsu; Tsukada, Hideo; Suzuki, Masaaki
Chemistry - A European Journal, 2009 , vol. 15, # 16 p. 4165 - 4171
反应条件
sodium periodate; ammonium acetate in water; acetone 48 h;
参考文献
Patil, Aditi S.; Mo, Dong-Liang; Wang, Heng-Yen; Mueller, Daniel S.; Anderson, Laura L.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 31 p. 7799 - 7803
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate in N,N-dimethyl-formamide
T=80°C; Suzuki-Miyaura coupling; 17 h; Inert atmosphere;
参考文献
Kondoh, Azusa; Jamison, Timothy F.
Chemical Communications, 2010 , vol. 46, # 6 p. 907 - 909
反应条件
1: 99 percent / NaOMe / PdCl2(PPh3)2 / methanol / 0.08 h / microwave irradiation
2: 97 percent / AcONa / ethanol / 1 h / 80 °C
3: 90 percent / various solvent(s) / 1 h / 180 °C / microwave irradiation
4: 86 percent / diethyl fumarate / Pd/C / diphenyl ether / 5 h / Heating
View Scheme
参考文献
Kumemura, Teppei; Choshi, Tominari; Yukawa, Junko; Hirose, Aya; Nobuhiro, Junko; Hibino, Satoshi
Heterocycles, 2005 , vol. 66, # 1 p. 87 - 90
