2-((叔丁氧基羰基)氨基)-2-苯乙酸甲酯合成路线 （共 38 条）
反应条件
potassium hydrogencarbonate in N,N-dimethyl-formamide
3 h; Ambient temperature;
参考文献
Matsunaga, Nobuyuki; Harada, Hiroshi; Aoyama, Toyohiko; Shioiri, Takayuki
Heterocycles, 1992 , vol. 33, # 1 p. 235 - 255
反应条件
1: ammonium cerium (IV) nitrate; water / acetonitrile / 0.5 h / 0 °C
2: acetonitrile / 12 h / 20 °C
3: acetic acid; sodium nitrite / dimethyl sulfoxide / 24 h / 40 °C / Inert atmosphere
4: diethyl ether / 0.5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Liu, Xiang-Wei; Yan, Yan; Wang, Yong-Qiang; Wang, Chao; Sun, Jian
Chemistry - A European Journal, 2012 , vol. 18, # 30 p. 9204 - 9207
反应条件
1: acetonitrile / 12 h / 20 °C
2: acetic acid; sodium nitrite / dimethyl sulfoxide / 24 h / 40 °C / Inert atmosphere
3: diethyl ether / 0.5 h / 20 °C / Inert atmosphere
View Scheme
参考文献
Liu, Xiang-Wei; Yan, Yan; Wang, Yong-Qiang; Wang, Chao; Sun, Jian
Chemistry - A European Journal, 2012 , vol. 18, # 30 p. 9204 - 9207
反应条件
potassium carbonate
3.5 h; Title compound not separated from byproducts.;
参考文献
Xu, Xuenong; Furukawa, Tomihiro; Okino, Tomotaka; Miyabe, Hideto; Takemoto, Yoshiji
Chemistry - A European Journal, 2006 , vol. 12, # 2 p. 466 - 476
反应条件
ammonium cerium(IV) nitrate
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Park, Yong Sun; Beak, Peter
Journal of Organic Chemistry, 1997 , vol. 62, # 6 p. 1574 - 1575
反应条件
in diethyl ether
Title compound not separated from byproducts.;
参考文献
Yokoyama; Hikawa; Murakami
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 12 p. 1431 - 1434
反应条件
in methanol; diethyl ether
参考文献
Mita, Tsuyoshi; Sugawara, Masumi; Hasegawa, Hiroyuki; Sato, Yoshihiro
Journal of Organic Chemistry, 2012 , vol. 77, # 5 p. 2159 - 2168
反应条件
1: LiCl, NaBH4 / tetrahydrofuran; ethanol / 1.) 0 deg C, 30 min, 2.) RT, 5 h
2: sulfur trioxide-pyridine complex (Py*SO3), triethylamine / dimethylsulfoxide; CH2Cl2 / 0.25 h / Ambient temperature
View Scheme
参考文献
Matsunaga, Nobuyuki; Harada, Hiroshi; Aoyama, Toyohiko; Shioiri, Takayuki
Heterocycles, 1992 , vol. 33, # 1 p. 235 - 255
