N-甲酰基-N-甲基苯甲酰胺合成路线 （共 16 条）
反应条件
titanium tetrachloride; triethylamine in dichloromethane
T=0 - 25°C; 2 h; Inert atmosphere;
参考文献
Liu, Yu; Li, Dan; Park, Cheol-Min
Angewandte Chemie - International Edition, 2011 , vol. 50, # 32 p. 7333 - 7336
反应条件
ozone in methanol
T=-78°C;
参考文献
Kashima, Choji; Harada, Kaori; Hosomi, Akira
Heterocycles, 1992 , vol. 33, # 1 p. 385 - 390
反应条件
1: N-methyl-benzamide With n-butyllithium in tetrahydrofuran; hexanes
T=0°C; 1 h; Inert atmosphere;
2: 1H-benzotriazole-1-carboxaldehyde in tetrahydrofuran; hexanes
T=0 - 20°C; 12 h; Inert atmosphere;
参考文献
Pasqua, Adele E.; Crawford, James J.; Long, De-Liang; Marquez, Rodolfo
Journal of Organic Chemistry, 2012 , vol. 77, # 5 p. 2149 - 2158
反应条件
benzoyl chloride in chloroform-d1
T=20°C;
参考文献
Boehme, Horst; Raude, Edgar
Chemische Berichte, 1981 , vol. 114, # 10 p. 3421 - 3429
反应条件
benzoyl chloride in chloroform-d1
T=20°C;
参考文献
Boehme, Horst; Raude, Edgar
Chemische Berichte, 1981 , vol. 114, # 10 p. 3421 - 3429
反应条件
1: chlorotrimethylsilane / 18 h / Heating
2: tetrahydrofuran / 12 h
3: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C
View Scheme
参考文献
Constantino, Luis; Iley, Jim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 13 p. 1894 - 1900
反应条件
1: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C
2: chlorotrimethylsilane / 18 h / Heating
3: tetrahydrofuran / 12 h
4: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C
View Scheme
参考文献
Constantino, Luis; Iley, Jim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 13 p. 1894 - 1900
反应条件
1: tetrahydrofuran / 12 h
2: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C
View Scheme
参考文献
Constantino, Luis; Iley, Jim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 13 p. 1894 - 1900
反应条件
1: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C
2: chlorotrimethylsilane / 18 h / Heating
3: tetrahydrofuran / 12 h
4: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C
View Scheme
参考文献
Constantino, Luis; Iley, Jim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 13 p. 1894 - 1900
反应条件
1: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C
2: chlorotrimethylsilane / 18 h / Heating
3: tetrahydrofuran / 12 h
4: t-BuOOH; 5,10,15,20-tetraphenylporphyrinatoiron(III) chloride / CH2Cl2 / 30 °C
View Scheme
参考文献
Constantino, Luis; Iley, Jim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 13 p. 1894 - 1900
