(3-氨基萘-2-基)甲醇合成路线 （共 6 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C;
参考文献
MERCK and CO., INC.
Patent: WO2007/81570 A2, 2007 ;
Location in patent: Page/Page column 45 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=5°C; 2 h;
参考文献
Taffarel, Emmanuelle; Chirayil, Sarah; Thummel, Randolph P.
Journal of Organic Chemistry, 1994 , vol. 59, # 4 p. 823 - 828
反应条件
1: 52 percent / 30percent aq. NH3, ZnCl2 / 36 h / 195 °C 2: 60 percent / conc. H2SO4 / Heating 3: 75 percent / LiAlH4 / tetrahydrofuran / 2 h / 5 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 4 p. 823 - 828
反应条件
lithium aluminium tetrahydride in diethyl ether 0.666667 h; RefluxInert atmosphere;
参考文献
Organometallics, , vol. 33, # 1 p. 61 - 68
反应条件
T=35 - 45°C; bei der elektrolytischen Reduktion;
参考文献
Archiv der Pharmazie (Weinheim, Germany), , p. 583
反应条件
1: 95 percent / Et3N / CHCl3 / 1.) 0 deg C, 1 h, 2.) r.t., overnight 2: 95 percent / MnO2 / CHCl3 / 24 h / Ambient temperature 3: 95 percent / 2 N aq. HCl / ethanol / 15 h / Heating View Scheme
参考文献
Taffarel, Emmanuelle; Chirayil, Sarah; Thummel, Randolph P.
Journal of Organic Chemistry, 1994 , vol. 59, # 4 p. 823 - 828
