4-[(叔丁基二苯基硅烷基)氧基]环己烷甲腈合成路线 (共 2 条)
反应条件
1: With oxalyl dichloride in dichloromethane; dimethyl sulfoxide T=-78°C; 0.25 h; 2: With triethylamine in dichloromethane; dimethyl sulfoxide T=-78 - 20°C; 2 h;
参考文献
US2008/58347 A1, ;
Page/Page column 62-63 ;
US 20080058347 A1
反应条件
in dichloromethane; water; N,N-dimethyl-formamide
参考文献
Lipha Lyonnaise Industrielle Pharmaceutique
Patent: US5387709 A1, 1995 ;