2-苯基哒嗪-3(2H)-酮合成路线 （共 7 条）
反应条件
caesium carbonate; hydroxybenzaldoxime; copper(I) oxide in acetonitrile T=82°C; 100 h;
参考文献
Cristau, Henri-Jean; Cellier, Pascal P.; Spindler, Jean-Francis; Taillefer, Marc
Chemistry - A European Journal, 2004 , vol. 10, # 22 p. 5607 - 5622
反应条件
T=550°C; P=0.01 - 0.1 Torr; 3 h;
参考文献
McNab, Hamish; Stobie, Ian
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 8 p. 1845 - 1854
反应条件
palladium on activated charcoal; ethanol Hydrogenation;
参考文献
Druey et al.
Helvetica Chimica Acta, 1954 , vol. 37, p. 510,520
反应条件
1: POCl3 2: palladium/charcoal; ethanol / Hydrogenation View Scheme
参考文献
Druey et al.
Helvetica Chimica Acta, 1954 , vol. 37, p. 510,520
反应条件
sodium hydride 1.) THF, 25 deg C, 2 h, 2.) THF, a.) 25 deg C, 1.5 h, b.) 65 deg C, 8 h; Yield given. Multistep reaction;
参考文献
Patel; Vyas; Pandey; Tavares; Fernandes
Synthetic Communications, 1991 , vol. 21, # 8-9 p. 1021 - 1026
反应条件
LiN(Cy)2 1.) THF, -78 deg C, 15 min, 2.) THF, from -78 deg C to 25 deg C, 4.5 h; Yield given. Multistep reaction;
参考文献
Patel; Vyas; Pandey; Tavares; Fernandes
Synthetic Communications, 1991 , vol. 21, # 18-19 p. 1935 - 1940
反应条件
Yield given. Multistep reaction;
参考文献
Schmitt, M.; Bourguignon, J. J.; Wermuth, C. G.
Tetrahedron Letters, 1990 , vol. 31, # 15 p. 2145 - 2148
