1: 40 percent / diphenyl-2-pyridylphosphine; di-tert-butyl azodicarboxylate / CH2Cl2 / 2 h / 20 °C 2: 94 percent / PhSH; potassium carbonate / acetonitrile / 50 °C View Scheme
参考文献
Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1049 - 1057
1: 74 percent / diphenyl-2-pyridylphosphine; di-tert-butyl azodicarboxylate / CH2Cl2 / 2 h / 20 °C
2: 90 percent / PhSH; potassium carbonate / acetonitrile / 50 °C
View Scheme
参考文献
Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1049 - 1057
1: 64 percent / diphenyl-2-pyridylphosphine; di-tert-butyl azodicarboxylate / CH2Cl2 / 2 h / 20 °C
2: 96 percent / PhSH; potassium carbonate / acetonitrile / 50 °C
View Scheme
参考文献
Guisado, Cristina; Waterhouse, Jodie E.; Price, Wayne S.; Jorgensen, Michael R.; Miller, Andrew D.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 6 p. 1049 - 1057