(R)-[1-[[[(4-甲基苯基)磺酰基]氧基]甲基]-2-苯基乙基]氨基甲酸1,1-二甲基乙酯合成路线 （共 22 条）
反应条件
pyridine in dichloromethane 12 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 36, # 14 p. 2505 - 2508
反应条件
1: 0.1 g / triethylamine / CH2Cl2 / 1 h / 0 °C 2: triethylamine / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 39 p. 9758 - 9763
反应条件
1: 0.1 g / triethylamine / CH2Cl2 / 1 h / 0 °C 2: triethylamine / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 39 p. 9758 - 9763
反应条件
1: 89 percent / LiBH4 / 1,2-dimethoxy-ethane 2: 89 percent / pyridine View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 24, # 5 p. 503 - 510
反应条件
1: 97 percent 2: 89 percent / LiBH4 / 1,2-dimethoxy-ethane 3: 89 percent / pyridine View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 24, # 5 p. 503 - 510
反应条件
1: 70 percent / Raney-Nickel; AcOH; hydrogen / methanol / 16 h / 20 °C / 3102.97 Torr 2: 0.1 g / triethylamine / CH2Cl2 / 1 h / 0 °C 3: triethylamine / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 39 p. 9758 - 9763
反应条件
1.1: D-proline / acetonitrile / 3 h / 0 - 20 °C 1.2: NaBH4 / acetonitrile; ethanol / 0.08 h / 0 °C 2.1: 70 percent / Raney-Nickel; AcOH; hydrogen / methanol / 16 h / 20 °C / 3102.97 Torr 3.1: 0.1 g / triethylamine / CH2Cl2 / 1 h / 0 °C 4.1: triethylamine / CH2Cl2 / 1 h / 0 °C View Scheme
参考文献
Tetrahedron, , vol. 63, # 39 p. 9758 - 9763
反应条件
1: NaBH4; I2 / tetrahydrofuran / 18 h / Heating 2: 95 percent / tetrahydrofuran; H2O / 1 h / 20 °C 3: 90 percent / pyridine / CH2Cl2 / 12 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 53, # 13 p. 4769 - 4778
反应条件
pyridine in chloroform 22 h; Yield given;
参考文献
Tetrahedron Letters, , vol. 40, # 13 p. 2629 - 2632
反应条件
1: LiAlH4 / tetrahydrofuran / 0 °C 2: pyridine / 0 °C View Scheme
参考文献
Chemistry Letters, , # 12 p. 2409 - 2412
