2-(2-溴苯基)-N-甲基乙酰胺合成路线 （共 5 条）
反应条件
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; 2 h;
参考文献
Young, Ha Kim; Lee, Hyuk; Yeong, Joon Kim; Bum, Tae Kim; Heo, Jung-Nyoung
Journal of Organic Chemistry, 2008 , vol. 73, # 2 p. 495 - 501
反应条件
triethylamine in water; acetone T=20°C; 1 h;
参考文献
Elban, Mark A.; Chapuis, Jean C.; Li, Mei; Hecht, Sidney M.
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 18 p. 6119 - 6125
参考文献
Sielecki, Thais M.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3673 - 3676
反应条件
copper(l) iodide; 1,10-phenanthroline; tetrabutylammomium bromide; potassium carbonate in toluene T=100°C; 8 h;
参考文献
Sun, Jie; Liu, Bingxin; Xu, Bin
RSC Advances, 2013 , vol. 3, # 17 p. 5824 - 5827
反应条件
1: LiAlH4 / 24 h / Heating
2: ammonium sulfate / 24 h / Heating
3: 60 percent / lithium diisopropylamide / pentane / -78 deg C to RT, overnight
View Scheme
参考文献
Sielecki, Thais M.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3673 - 3676
