反应条件
1: LiAlH4 / 24 h / Heating
2: ammonium sulfate / 24 h / Heating
3: 1) LiBr, 2) sec-butyllithium / 1) THF, 30 min, RT, 2) THF, -78 deg C, 10 min
View Scheme
参考文献
Sielecki, Thais M.; Meyers, A. I.
Journal of Organic Chemistry, 1992 , vol. 57, # 13 p. 3673 - 3676
