2-BOC-八氢吡咯基[3,4-C]吡咯合成路线 （共 5 条）
反应条件
hydrogen; palladium(II) hydroxide/carbon in methanol T=50°C; P=3102.97 Torr; 2.5 h;
参考文献
Basha, Anwer; Bunnelle, William H.; Dart, Michael J.; Gallagher, Megan E.; Ji, Jianguo; Li, Tao; Pace, Jennifer M.; Ryther, Keith B.; Tietje, Karin R.; Mortell, Kathleen H.; Nersesian, Diana L.; Schrimpf, Michael R.
Patent: US2005/101602 A1, 2005 ;
Location in patent: Page/Page column 28 ;
反应条件
1: dichloromethane / 24 h / 23 °C 2: hydrogen / palladium 10 on activated carbon / acetic acid; methanol / 72 h / 3620.13 Torr View Scheme
参考文献
WO2011/50198 A1, ;
WO 2011/050198 A1
反应条件
1: dichloromethane / 24 h / 23 °C 2: hydrogen / palladium 10 on activated carbon / acetic acid; methanol / 72 h / 3620.13 Torr View Scheme
参考文献
WO2011/50198 A1, ;
WO 2011/050198 A1
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / -5 °C / |Reflux 2: dichloromethane / 0 - 20 °C 3: hydrogen; palladium(II) oxide hydrate / methanol View Scheme
反应条件
hydrogenchloride in 1,4-dioxane
参考文献
BAYER AKTIENGESELLSCHAFT
Patent: WO2003/106450 A1, 2003 ;
Location in patent: Page column 54 ;
WO 03/106450 A1
