2-氨基吡啶 N-氧化物合成路线 （共 34 条）
反应条件
tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,4-dioxane T=110°C; 42 h; Inert atmosphere;
参考文献
Wolinska, Ewa
Heterocyclic Communications, 2012 , vol. 18, # 5-6 p. 227 - 232
反应条件
potassium carbonate in N,N-dimethyl-formamide T=140°C; 5 h;
参考文献
Rykowski; Pucko
Polish Journal of Chemistry, 1998 , vol. 72, # 11 p. 2378 - 2383
反应条件
potassium carbonate T=175°C;
参考文献
Rykowski; Pucko
Polish Journal of Chemistry, 1998 , vol. 72, # 11 p. 2378 - 2383
反应条件
potassium carbonate T=170 - 175°C; 0.25 h;
参考文献
Rykowski; Pucko
Polish Journal of Chemistry, 1998 , vol. 72, # 11 p. 2378 - 2383
反应条件
n-Pentyl nitrite in acetic acid
1 h;
参考文献
Saeki, Seitaro; Kondo, Sachiko; Hayashi, Takaaki; Hamana, Masatomo
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 5 p. 1780 - 1789
反应条件
in acetonitrile
T=60°C; 24 h;
参考文献
Rival; Taudou; Ecalle
Farmaco, 1993 , vol. 48, # 6 p. 857 - 869
参考文献
Katritzky
Journal of the Chemical Society, 1957 , p. 191,197
反应条件
1: 55 percent / KI / dimethylformamide / 3 h / Heating
2: 65 percent / PCl3 / ethyl acetate / 3 h / Heating
View Scheme
参考文献
Kalinowski, Jerzy; Rykowski, Andrzej; Nantka-Namirski, Pawel
Polish Journal of Chemistry, 1984 , vol. 58, # 1-3 p. 125 - 134
反应条件
1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C / |Sealed tube
2: tetrahydroxydiboron / 0.17 h
View Scheme
参考文献
Londregan, Allyn T.; Piotrowski, David W.; Xiao, Jun
Synlett, 2013 , vol. 24, # 20 art. no. ST-2013-S0695-L, p. 2695 - 2700
参考文献
Katritzky
Journal of the Chemical Society, 1957 , p. 191,197
