1,3-双(2,4,6-三甲基苯基)氯化咪唑合成路线 （共 6 条）
反应条件
in tetrahydrofuran T=40°C;
参考文献
Thomson, Jennifer E.; Campbell, Craig D.; Concellon, Carmen; Duguet, Nicolas; Rix, Kathryn; Slawin, Alexandra M. Z.; Smith, Andrew D.
Journal of Organic Chemistry, 2008 , vol. 73, # 7 p. 2784 - 2791
反应条件
hydrogenchloride in 1,4-dioxane; ethyl acetate T=0°C; 2.5 h; Product distribution / selectivity;
参考文献
UNIVERSITY OF NEW ORLEANS RESEARCH AND TECHNOLOGY FOUNDATION, INC.
Patent: WO2008/36084 A1, 2008 ;
Location in patent: Page/Page column 4; 6; 7-8 ;
反应条件
1: in toluene T=20°C; 0.5 h; Inert atmosphere; 2: With N-Trimethylamine hydrochloride in toluene
参考文献
Jana, Anukul; Tavcar, Gasper; Roesky, Herbert W.; Schulzke, Carola
Dalton Transactions, 2010 , vol. 39, # 27 p. 6217 - 6220
反应条件
1: 80 percent / propan-1-ol; H2O / 23 - 60 °C 2: 40 percent / tetrahydrofuran / 120 h / 23 °C View Scheme
参考文献
Tetrahedron, , vol. 55, # 51 p. 14523 - 14534
反应条件
1: 1,3-bis(2,4,6-trimethylphenyl)imidazolinium chloride With potassium 2-methyl-2-butoxide in hexane; toluene T=50°C; 0.166667 h; 2: Fuuml;rstner's ruthenium indenylidene catalyst in hexane; toluene T=50°C; 15 h;
参考文献
Puentener, Kurt; Scalone, Michelangelo
Patent: US2006/241156 A1, 2006 ;
Location in patent: Page/Page column 6 ;
反应条件
potassium tert-butylate in tetrahydrofuran 0.333333 h; Ambient temperature;
参考文献
Arduengo III, Anthony J.; Rasika Dias; Harlow, Richard L.; Kline, Michael
Journal of the American Chemical Society, 1992 , vol. 114, # 14 p. 5530 - 5534
