5-O-叔丁基联苯基硅烷-2,3-O-异亚丙基-Alpha,β-D-呋喃核合成路线 （共 4 条）
反应条件
1: 2,3-O-Isopropylidene-D-ribose With 1H-imidazole in dichloromethane T=0°C; 0.5 h; Inert atmosphere; 2: tert-butylchlorodiphenylsilane in dichloromethane T=20°C; 8 h; Inert atmosphere;
参考文献
Srihari; Sathish Reddy; Yadav; Yedlapudi; Kalivendi, Shasi V.
Tetrahedron Letters, 2013 , vol. 54, # 41 p. 5616 - 5618
反应条件
1.1: sulfuric acid / 24 h / 20 °C / |Inert atmosphere 2.1: 1H-imidazole / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 2.2: 8 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 41 p. 5616 - 5618
反应条件
1: 2,3-O-Isopropylidene-D-ribose With 1H-imidazole in dichloromethane
T=0°C; 0.5 h; Inert atmosphere;
2: tert-butylchlorodiphenylsilane in dichloromethane
T=20°C; 8 h; Inert atmosphere;
参考文献
Srihari; Sathish Reddy; Yadav; Yedlapudi; Kalivendi, Shasi V.
Tetrahedron Letters, 2013 , vol. 54, # 41 p. 5616 - 5618
反应条件
1.1: sulfuric acid / 24 h / 20 °C / |Inert atmosphere
2.1: 1H-imidazole / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere
2.2: 8 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Srihari; Sathish Reddy; Yadav; Yedlapudi; Kalivendi, Shasi V.
Tetrahedron Letters, 2013 , vol. 54, # 41 p. 5616 - 5618
