反应条件
1: phenyllithium With 3-butyl-1,1-diethyl-1,3-dihydrobenzo[c][1,2]oxasilole in tetrahydrofuran; anhydrous butyl ether
T=-78 - 20°C; Inert atmosphere;
2: azepan-1-yl benzoate With copper(l) iodide; dpca in tetrahydrofuran; anhydrous butyl ether
T=20°C; 2 h; Inert atmosphere;
参考文献
Nguyen, Minh H.; Smith, Amos B.
Organic Letters, 2013 , vol. 15, # 18 p. 4872 - 4875