hydrogen; platinum(IV) oxide in ethanol P=2584.17 Torr; 0.333333 h;

1.1: potassium carbonate / butanone / 0.5 h / 20 °C 1.2: 12 h / 78 - 82 °C 2.1: hydrogen / palladium 10 on activated carbon / ethyl acetate / 25 - 35 °C View Scheme

1.1: potassium carbonate / butanone / 0.5 h / 20 °C 1.2: 12 h / 78 - 82 °C 2.1: hydrogen / palladium 10 on activated carbon / ethyl acetate / 25 - 35 °C View Scheme

1.1: AlCl3, aluminium chloride / chlorobenzene / 2 h / 25 °C / Reflux 2.1: AlCl3, aluminium chloride / chlorobenzene / 2 h / 75 °C 2.2: 0.5 h / 5 - 65 °C 3.1: potassium carbonate / butanone / 20 h / 85 °C 3.3: 0.5 h / 25 - 65 °C 4.1: potassium carbonate / toluene; water 5.1: hydrogen / Raney Nickel / methanol / 8 h / 55 °C / 3677.86 Torr 5.2: 0.5 h / 25 - 65 °C 6.1: potassium carbonate / toluene; water / 1 h / 35 °C View Scheme

1.1: AlCl3, aluminium chloride / chlorobenzene / 2 h / 25 °C / Reflux 2.1: AlCl3, aluminium chloride / chlorobenzene / 2 h / 75 °C 2.2: 0.5 h / 5 - 65 °C 3.1: potassium carbonate / butanone / 20 h / 85 °C 3.3: 0.5 h / 25 - 65 °C 4.1: potassium carbonate / toluene; water 5.1: hydrogen / Raney Nickel / methanol / 8 h / 55 °C / 3677.86 Torr 5.2: 0.5 h / 25 - 65 °C 6.1: potassium carbonate / toluene; water / 1 h / 35 °C View Scheme

1.1: AlCl3, aluminium chloride / chlorobenzene / 2 h / 75 °C 1.2: 0.5 h / 5 - 65 °C 2.1: potassium carbonate / butanone / 20 h / 85 °C 2.3: 0.5 h / 25 - 65 °C 3.1: potassium carbonate / toluene; water 4.1: hydrogen / Raney Nickel / methanol / 8 h / 55 °C / 3677.86 Torr 4.2: 0.5 h / 25 - 65 °C 5.1: potassium carbonate / toluene; water / 1 h / 35 °C View Scheme

1: phosphorous pentoxide / 1.25 h / 35 °C / Inert atmosphere; Large scale reaction 2: tetrabutylammomium bromide; potassium iodide / N,N-dimethyl-formamide / 14 h / 85 °C 3: methylamine / water; isopropyl alcohol / 1 h / 75 °C 4: isopropyl alcohol / 1.5 h / 5 - 65 °C / Large scale reaction 5: sodium hydrogencarbonate / dichloromethane; water / 0.5 h View Scheme

1.1: sodium hydrogencarbonate / water; toluene / 0.5 h / Large scale reaction 1.2: 1.5 h / Reflux 2.1: tin(IV) chloride / dichloromethane / 1 h / 0 - 25 °C 3.1: tetrabutylammomium bromide; potassium iodide / N,N-dimethyl-formamide / 14 h / 85 °C 4.1: methylamine / water; isopropyl alcohol / 1 h / 75 °C 5.1: isopropyl alcohol / 1.5 h / 5 - 65 °C / Large scale reaction 6.1: sodium hydrogencarbonate / dichloromethane; water / 0.5 h View Scheme

1: methylamine / water; isopropyl alcohol / 1 h / 75 °C 2: isopropyl alcohol / 1.5 h / 5 - 65 °C / Large scale reaction 3: sodium hydrogencarbonate / dichloromethane; water / 0.5 h View Scheme

1: tetrabutylammomium bromide; potassium iodide / N,N-dimethyl-formamide / 14 h / 85 °C 2: methylamine / water; isopropyl alcohol / 1 h / 75 °C 3: isopropyl alcohol / 1.5 h / 5 - 65 °C / Large scale reaction 4: sodium hydrogencarbonate / dichloromethane; water / 0.5 h View Scheme