2,2,7,8-四甲基-6-色满醇合成路线 （共 6 条）
反应条件
perchloric acid; hydrogen; palladium on activated charcoal in ethanol T=20°C; Reduction; P=53200 Torr; 6 h;
参考文献
Yenes, Susana; Messeguer, Angel
Tetrahedron, 1999 , vol. 55, # 49 p. 14111 - 14122
反应条件
1: With formic acid in tetrahydrofuran 3 h; Reflux; 2: With hydrogenchloride; methanol in water 0.333333 h; Reflux;
参考文献
Kloser, Elisabeth; Boehmdorfer, Stefan; Brecker, Lothar; Kaehlig, Hanspeter; Netscher, Thomas; Mereiter, Kurt; Rosenau, Thomas
European Journal of Organic Chemistry, 2011 , # 13 p. 2450 - 2457
反应条件
boron trifluoride diethyl etherate in 1,4-dioxane 5 h; Heating / reflux;
参考文献
Walkinshaw, Gail; Bodupalli, Sekhar; Wang, Bing; Miller, Guy
Patent: US2005/65099 A1, 2005 ;
Location in patent: Page 17 ;
反应条件
toluene-4-sulfonic acid in toluene T=100°C; 18 h;
参考文献
Hong, Mei Peng; Webster, Richard D.
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2169 - 2175
反应条件
1: 60 percent / methanesulfonic acid / 1 h / 90 °C 2: 90 percent / aq. HClO4; H2 / Pd/C / ethanol / 6 h / 20 °C / 53200 Torr View Scheme
参考文献
Yenes, Susana; Messeguer, Angel
Tetrahedron, 1999 , vol. 55, # 49 p. 14111 - 14122
反应条件
1: 60 percent / methanesulfonic acid / 1 h / 90 °C 2: 90 percent / aq. HClO4; H2 / Pd/C / ethanol / 6 h / 20 °C / 53200 Torr View Scheme
参考文献
Yenes, Susana; Messeguer, Angel
Tetrahedron, 1999 , vol. 55, # 49 p. 14111 - 14122
