5,10,15,20-四苯基-21H,23H-卟吩镍(II)合成路线 （共 18 条）
反应条件
sodium acetate; potassium carbonate in N,N-dimethyl-formamide; chlorobenzene T=150°C;
参考文献
Yao, Shu A.; Hansen, Christopher B.; Berry, John F.
Polyhedron, 2013 , vol. 58, p. 2 - 6
反应条件
pyridine; hydrazine hydrate T=115°C; 3 h;
参考文献
Akhigbe, Joshua; Samankumara, Lalith P.; Brueckner, Christian
Tetrahedron Letters, 2012 , vol. 53, # 27 p. 3524 - 3526
反应条件
bis(acetylacetonate)nickel(II) in toluene 24 h; DarknessReflux;
参考文献
He, Chao; He, Qingguo; Deng, Changmin; Shi, Liqi; Zhu, Defeng; Fu, Yanyan; Cao, Huimin; Cheng, Jiangong
Chemical Communications, 2010 , vol. 46, # 40 p. 7536 - 7538
反应条件
in solid High Pressure; 2000 MPa at room temp.; extrd. (chloroform), chromy.(alumina); UV;
参考文献
Zhorin, V. A.; Nikiforov, G. A.; Khristyuk, A. L.; Enikolopyan, N. S.
Doklady Physical Chemistry (Translation of the physical chemistry section of Doklady Akademii Nauk), 1983 , vol. 271, p. 510 - 512
Doklady Akademii Nauk SSSR, 1983 , vol. 271, p. 650 - 652
反应条件
sodium carbonate in water T=349.84°C; 1 h; AutoclaveInert atmosphere;
参考文献
Sato, Takafumi; Ebisawa, Katsutoshi; Ito, Satoshi; Sue, Kiwamu; Itoh, Naotsugu
Chemistry Letters, 2011 , vol. 40, # 12 p. 1414 - 1416
反应条件
in pyridine other Radiation; porphyrin, metal salt and pyridine were sealed in a glass tube, microwave power of 300 W, heated from room temp. to 180°C, stirred for 15min, cooled to 50°C; vessel was opened, decanted, TLC (silica gel), UV;
参考文献
Dean, Michelle L.; Schmink, Jason R.; Leadbeater, Nicholas E.; Brueckner, Christian
Dalton Transactions, 2008 , # 10 p. 1341 - 1345
反应条件
H2O; CF3COOH; 2,3-dichloro-5,6-dicyano-1,4-benzoquinone in dichloromethane treating with CF3COOH for 2 h; oxidation with DDQ for 1 h; metallation with Ni(acac)2;
参考文献
Angewandte Chemie - International Edition, , vol. 46, # 13 p. 2306 - 2309
反应条件
in pyridine Irradiation (UV/VIS); soln. of Ni complex in C5H5N excited with 406.7-nm laser; not isolated, monitored by Raman spectroscopy;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 2099 - 2100
反应条件
in further solvent(s) Irradiation (UV/VIS); soln. of Ni complex in C5H10NH excited with 406.7-nm laser; not isolated, monitored by Raman spectroscopy;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 2099 - 2100
反应条件
in dichloromethane inert atmosphere; > 1 d; not isolated; detd. by UV-VIS, ESR and resonance Raman spectroscopy;
参考文献
Inorganic Chemistry, , vol. 34, p. 2201 - 2206
