5,10,15,20-四苯基-21H,23H-卟吩镍(II)合成路线 （共 18 条）
反应条件
in dichloromethane inert atmosphere; 30 min; not isolated; detd. by UV-VIS, ESR and resonance Raman spectrosco;
参考文献
Inorganic Chemistry, , vol. 34, p. 2201 - 2206
反应条件
in dichloromethane inert atmosphere; in presence of pyridine; > 6-10 h; not isolated; detd. by UV-VIS, ESR and resonance Raman spectrosco;
参考文献
Inorganic Chemistry, , vol. 34, p. 2201 - 2206
反应条件
in dichloromethane inert atmosphere; >= 1 d; not isolated; detd. by UV-VIS, ESR and resonance Raman spectroscopy;
参考文献
Inorganic Chemistry, , vol. 34, p. 2201 - 2206
反应条件
in N,N-dimethyl-formamide excess nickel(II) acetate, refluxing; drying, chromy. (alumina, silica gel, CH2Cl2 or CHCl3), recrystn. (toluene/ethanol);
参考文献
Journal of Chemical Physics, , vol. 89, # 11 p. 6567 - 6576
反应条件
in further solvent(s) Kinetics; Irradiation (UV/VIS); photodissocn. by laser exitation; detected by XAFS;
参考文献
Journal of Electron Spectroscopy and Related Phenomena, , vol. 119, # 2-3 p. 161 - 174
反应条件
in N,N-dimethyl-formamide react. of starting compd. in DMF according to A. D. Adler and F. R. Longo; J. Inorg. Nucl. Chem. 32, 2443 (1970); react. is monitored by thin-layer chromy., purifn. of Ni-complex by chromy. (Al2O3, CHCl3), slow recrystn. from CH2Cl2; characterized by UV and mass spectroscopy;
参考文献
Berichte der Bunsen-Gesellschaft, , vol. 96, # 6 p. 821 - 833
反应条件
in dimethyl sulfoxide Kinetics; at 298-363 K;
参考文献
Russian Journal of General Chemistry, , vol. 70, # 8 p. 1299 - 1303
反应条件
in isopropyl alcohol; acetone; toluene Kinetics; other Radiation; room temp.; not isolated, IR and UV/VIS monitoring;
参考文献
Journal of Physical Chemistry, , vol. 98, # 17 p. 4617 - 4621
