反应条件
1: palladium 10 on activated carbon; hydrogen / methanol / 20 °C / |Inert atmosphere
2: 1,1-dimethylnitroethane; trimethylsilylazide / acetonitrile / 2 h / 20 °C / |Inert atmosphere; |Cooling
3: FeBr2 / toluene / 16 h / 140 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Nguyen, Quyen; Nguyen, Tuyen; Driver, Tom G.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 620 - 623
